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Beilstein J. Org. Chem. 2018, 14, 430–435, doi:10.3762/bjoc.14.31
Graphical Abstract
Scheme 1: The influence of the milling frequency on the reaction of 1a with NIS.
Scheme 2: Palladium-catalyzed ortho-iodination of 1a in toluene.
Scheme 3: Plausible mechanism.
Scheme 4: Palladium-catalyzed ortho-bromination and chlorination of 1a in a ball mill.